The Application of Polychalcogenide Salts to the Exploratory Synthesis of Solid State Multinary Chalcogenides at Intermediate Temperatures
1995; Wiley; Linguagem: Inglês
10.1002/9780470166444.ch2
ISSN1934-483X
AutoresMercouri G. Kanatzidis, Anthony C. Sutorik,
Tópico(s)Synthesis and characterization of novel inorganic/organometallic compounds
ResumoThe Application of Polychalcogenide Salts to the Exploratory Synthesis of Solid State Multinary Chalcogenides at Intermediate Temperatures Mercouri G. Kanatzidis, Mercouri G. Kanatzidis Department of Chemistry and Center for Fundamental Materials Research, Michigan State University, East Lansing, MichiganSearch for more papers by this authorAnthony C. Sutorik, Anthony C. Sutorik Department of Chemistry and Center for Fundamental Materials Research, Michigan State University, East Lansing, MichiganSearch for more papers by this author Mercouri G. Kanatzidis, Mercouri G. Kanatzidis Department of Chemistry and Center for Fundamental Materials Research, Michigan State University, East Lansing, MichiganSearch for more papers by this authorAnthony C. Sutorik, Anthony C. Sutorik Department of Chemistry and Center for Fundamental Materials Research, Michigan State University, East Lansing, MichiganSearch for more papers by this author Book Editor(s):Kenneth D. Karlin, Kenneth D. Karlin Department of Chemistry, The Johns Hopkins University, Baltimore, MarylandSearch for more papers by this author First published: 01 January 1995 https://doi.org/10.1002/9780470166444.ch2Citations: 151Book Series:Progress in Inorganic Chemistry AboutPDFPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Summary This chapter contains sections titled: Introduction The Nature of the Polychalcogenide Flux High-Temperature Reactions (> 600°C) Intermediate Temperature Reactions (200-600°C) in Ternary Systems (A/M/Q) with A2Qx Fluxes Aucuse4: Making Ternaries in A2Qx that do not Incorporate A+ Intermediate Temperature Reactions (200-600°C) in Quaternary Systems Reactions in Organic Cation-Polychalcogenide Salts Conclusions and Outlook Citing Literature References For a recent review see M. L. Steigerwald, in Inorganometallic Chemistry, T. P. Fehlner, Ed., Plenum, New York, 1992, pp. 333– 356. (a) C. Niu and C. M. Lieber, J. Am. Chem. Soc., 114, 3570 (1992). (b) T. Novet and D. Johnson, J. Am. Chem. Soc., 113, 3398 (1991). (a) C. J. Warren, S. S. Dhingra, R. C. Haushalter, and A. B. Bocarsley, J. Solid State Chem., 112, 340 (1994) (b) C. J. Warren, D. M. Ho, R. C. Haushalter, and A. B. Bocarsley, J. Chem. Soc. Chem. Commun., 361 (1994). A. Rabenau, Angew. Chem. Int. Ed. Engl., 24, 1026 (1985). R. M. Barrer, Hydrothermal Chemistry of Zeolites, Academic, New York, 1982. R. C. Haushalter and L. A. Mundi, Chem. Mater., 4, 31 (1992). (a) R. E. Morris, A. P. Wilkinson, and A. K. Cheetham, Inorg. Chem., 31, 4774 (1992). (b) W. T. A. Harrison, G. D. Stucky, R. E. Morris, and A. K. Cheetham, Acta Crystallogr. Ser. C, 48, 1365 (1992). (c) R. E. Morris, W. T. A. Harrison, G. D. Stucky, and A. K. Cheetham, J. Solid State Chem., 94, 227 (1991). (d) W. T. A. Harrison, R. E. Morris, and A. K. Cheetham, Acta Crystallogr. Ser. C, 48, 1182 (1992). (e) R. E. Morris, J. A. Hriljac, and A. K. Cheetham, Acta Crystallogr. Ser. C, 46, 2013 (1990). (f) R. E. Morris and A. K. Cheetham, Chem. Mater., 6, 67 (1994). (g) W. T. A. Harrison, G. D. Stucky, and A. K. Cheetham, Eur. J. Solid State Inorg. Chem., 30, 347 (1993). (a) M. I. Khan, Q. Chen, J. Zubieta, and D. P. Goshorn, Inorg. Chem., 31, 1556 (1992). (b) M. I. Khan, Q. Chen, and J. Zubieta, J. Chem. Soc. Chem. Commun., 305 (1992). (c) M. I. Khan, Q. Chen, D. P. Goshorn, H. Hope, S. Parkin, and J. Zubieta, J. Am. Chem. Soc., 114, 3341 (1992). (d) M. I. Khan and J. Zubieta, J. Am. Chem. Soc., 114, 10058 (1992). (e) M. I. Khan, Q. Chen, D. P. Goshorn, and J. Zubieta, Inorg. Chem., 33, 672 (1993). (a) J.-H. Liao and M. G. Kanatzidis, Inorg. Chem., 31, 431 (1992). (b) K.-W. Kim and M. G. Kanatzidis, J. Am. Chem. Soc., 114, 4878 (1992). P. T. Wood, W. T. Pennington, and J. W. Kolis, J. Am. Chem. Soc., 114, 9233 (1992). D. Elwell and H. J. Scheel, Crystal Growth from High-Temperature Solutions, Academic, New York, 1975. (a) R. R. Chianelli, T. A. Pecoraro, T. R. Halbert, W.-H. Pan, and E. I. Stiefel, J. Catal., 86, 226 (1984). (b) T. A. Pecoraro and R. R. Chianelli, J. Catal., 67, 430 (1981). (c) S. Harris and R. R. Chianelli, J. Catal., 86, 400 (1984). (a) H. Eckert, Angew. Chem. Int. Ed. Engl., 28, 1723 (1989). (b) R. Zallen, Physics of Amorphous Solids, Wiley, New York, 1983. (c) D. Strand and D. Adler, Proc. SPIE Int. Soc. Opt. Eng., 420, 200 (1983). (d) N. Yamada, N. Ohno, N. Akahira, K. Nishiuchi, K. Nagata, and M. Takeo, Proc. Int. Symp. Opt. Memory 1987, J. Appl. Phys., 26 (Suppl. 26–4), 61 (1987). (a) M. S. Whittingham, in Solid State Ionic Devices July 18–23 1988 Singapore, B. V. R. Chowdari and S. Radhakrishna, Eds., World Scientific, Singapore, 1988, pp. 55– 74. (b) W. L. Bowen, L. H. Burnette, and D. L. DeMuth, J. Electrochem. Soc., 136, 1614 (1989). (c) D. W. Murphy and F. A. Trumbore, J. Electrochem. Soc., 123, 960 (1976). (a) A. P. Brown, J. Electrochem. Soc., 134, 2506 (1987). (b) J. L. Sudworth and A. R. Tilley, in The Sulfur Electrode, Fused Salts and Solid Electrolytes, R. P. Tischer, Ed., Academic, New York, 1983, p. 235. (c) A. P. Brown, J. Electrochem. Soc., 134, 1921 (1987). (d) M. Liu and L. C. DeJonghe, J. Electrochem. Soc., 135, 741 (1988). (e) H. Yamin, A. Gorenshtein, J. Penciner, Y. Sternberg, and E. Peled, J. Electrochem. Soc., 135, 1045 (1988). (f) R. Knödler, J. App. Electrochem., 18, 653 (1988). (g) K. E. Heusler, A. Grzegorzewski, and R. Knödler, J. Electrochem. Soc., 140, 426 (1993). (a) H. J. Möller, Semiconductors for Solar Cells, Artech House, Boston, MA, 1993. (b) K. Zweibel, Basic Photovoltaic Principles and Methods, Van Nostrand-Reinhold, New York, 1984. (c) J. H. Armstrong, C. O. Pistole, M. S. Misra, V. K. Kapur, and B. M. Basol, in Space Photovoltaics Research and Technology 1991, NASA Conference Publication 3121, NASA, Washington DC, 1991, pp. 19–1– 19–8. (a) D. M. Rowe and C. M. Bhandari, Modern Thermoelectrics, Holt, Rinehart, and Winston, London, UK, 1983, p. 103. (b) K. Borkowski and J. Pyzyluski, J. Mater. Res. Bull., 22, 381 (1987). H. J. Scheel, J. Cryst. Growth, 24/25, 669 (1974). (a) R. Sanjines, H. Berger, and F. Levy, Mater. Res. Bull., 23, 549 (1988). (b) R. W. Garner and W. B. White, J. Cryst. Growth, 7, 343 (1970). S. A. Sunshine, D. Kang, and J. A. Ibers, J. Am. Chem. Soc., 109, 6202 (1987). (a) The Sodium-Sulfur Battery, J. L. Sudworth and A. R. Tilley, Eds., Chapman & Hall, New York, 1985. (b) W. Fischer, Mater. Res. Soc. Symp. Proc., 135, 541 (1989). (c) R. W. Powers and B. R. Karas, J. Electrochem. Soc., 136, 2787 (1989). (a) T. G. Pearson and P. L. Robinson, J. Chem. Soc., 1304 (1931). (b) G. H. Mathewson, J. Am. Chem. Soc., 29, 867 (1907). (c) W. Klemm, H. Sodomann, and P. Langmesser, Z. Anorg. Allg. Chem., 241, 281 (1939). (d) Gmelin's Handbuch der Anorganischen Chemie, Verlag Chemie, Weiheim/Brgstr, FRG, 1966. Soduim, Suppl. Part 3, pp. 1202– 1205 and references cited therein. (a) R. J. H. Clark and D. G. Cobbold, Inorg. Chem., 17, 3169 (1978). (b) P. Dubois, J. P. Lelieur, and G. Lepourte, Inorg. Chem., 27, 73 (1988). (c) K. W. Sharp and W. H. Koeheler, Inorg. Chem., 16, 2258 (1977). (d) L. Schultz and W. H. Koeheler, Inorg. Chem., 26, 1989 (1987). (a) R. W. M. Wardle, S. Bhaduri, C. N. Chau, and J. A. Ibers, Inorg. Chem., 27, 1747 (1988). (b) W. A. Herrmann, J. Rohrmann, E. Herdtweck, C. Hecht, M. L. Ziegler, and O. Serhadi, J. Organomet. Chem., 314, 295 (1986). (c) L. Y. Coh, C. Wei, and E. Sinn, J. Chem. Soc. Chem. Commun., 462 (1985). (d) A. L. Rheingold, C. M. Bolinger, and T. B. Rauchfuss, Acta Crystallogr. Ser. C, 42, 1878 (1986). (e) D. M. Giolando, M. Papavassiliou, J. Pickardt, and T. B. Rauchfuss, Inorg. Chem., 27, 2596 (1988). (f) B. W. Eichhorn, R. C. Haushalter, F. A. Cotton, and B. Wilson, Inorg. Chem., 27, 4084 (1988). (g) R. C. Haushalter, Angew. Chem. Int. Ed. Engl., 24, 433 (1985). (h) P. M. Fritz, W. Beck, U. Nagel, K. Polborn, W. A. Hermann, C. Hecht, and J. Rohmann, Z. Naturforsch., 43B, 665 (1988). (i) O. Scheidsteger, G. Huttner, K. Dehnicke, and J. Pebler, Angew. Chem. Int. Ed. Engl., 24, 428 (1985). (j) M. G. Kanatzidis and S.-P. Huang, Inorg. Chem., 30, 3572 (1991). (k) M. G. Kanatzidis and S. Dhingra, Inorg. Chem., 28, 2024 (1989). (l) M. G. Kanatzidis and S.-P. Huang, Inorg. Chem., 28, 4667 (1989). (m) H. Strasdeit, B. Krebs, and G. Henkel, Inorg. Chim. Acta, 89, L11 (1984). (o) M. G. Kanatzidis and S. Dhingra, unpublished results. (o) M. G. Kanatzidis and S.-P. Huang, Angew. Chem. Int. Ed. Engl., 28, 1513 (1989). (p) M. G. Kanatzidis and S.-P. Huang, Inorg. Chem., 30, 1455 (1991). F. Feher, in Handbuch der Praparativen Anorganischen Chemie, G. Brauer, Ed., Ferdinand Enke, Stuttgart, Germany, 1954, pp. 280– 281. S. Schreiner, L. E. Aleandri, D. Kang, and J. A. Ibers, Inorg. Chem., 28, 392 (1989). D. Coucouvanis and A. Hadjikyriacou, Inorg. Chem., 26, 1 (1987). J. M. Manoli, C. Potvin, and F. Secheresse, Inorg. Chem., 26, 340 (1987). K. O. Klepp, Z. Naturforsch., 47b, 937 (1992). P. M. Keane and J. A. Ibers, Acta Crystallogr. Ser. C, 48, 1301 (1992). P. M. Keane and J. A. Ibers, Inorg. Chem., 30, 1327 (1991). P. Böttcher, Angew. Chem. Int. Ed. Engl., 27, 759 (1988). L. Brattas and A. Kjekshus, Acta Chem. Scand., 26, 1 (1972). P. Wu, Y.-J. Lu, and J. A. Ibers, J. Solid State Chem., 97, 383 (1992). Y.-J. Lu and J. A. Ibers, Inorg. Chem., 30, 3317 (1991). Y.-J. Lu and J. A. Ibers, J. Solid State Chem., 94, 381 (1991). Y.-J. Lu and J. A. Ibers, J. Solid State Chem., 107, 58 (1993). Y.-J. Lu and J. A. Ibers, J. Solid State Chem., 98, 312 (1992). F. Jellinek, Ark. Kemi., 20, 447 (1963). F. Jellinek, Int. Rev. Sci. Inorg. Chem. Ser. One, 5, 351 (1972). (a) M. Latroche and J. A. Ibers, Inorg. Chem., 29, 1503 (1990). (b) H. Yun, C. R. Randall, and J. A. Ibers, J. Solid State Chem., 76, 109 (1988). L. E. Rendon-Diazmiron, C. F. Campana, and H. Steinfink, J. Solid State Chem., 47, 322 (1983). M. F. Mansuetto, P. M. Keane, and J. A. Ibers, J. Solid State Chem., 101, 257 (1992). M. F. Mansuetto, P. M. Keane, and J. A. Ibers, J. Solid State Chem., 105, 580 (1993). P. Matkovic and K. Schubert, J. Less-Common Met., 52, 217 (1977). R. Hoffman, Angew. Chem. Int. Ed. Engl., 26, 846 (1987). E. A. Axtell and M. G. Kanatzidis, manuscript in preparation. P. Wu and J. A. Ibers, J. Solid State Chem., 107, 347 (1993). (a) S. Furuseth, L. Brattas, and A. Kjekshus, Acta Chem. Scand., A29, 623 (1975). (b) H. Hahn and B. Harder, Z. Anorg. Allg. Chem., 288, 257 (1956). (c) J. Huster, Z. Naturforsh., B Anorg. Chem., Org. Chem., 35B, 775 (1980). (d) H. Hahn and B. Harder, Z. Anorg. Allg. Chem., 288, 241 (1956). D. Kang and J. A. Ibers, Inorg. Chem., 27, 549 (1988). Y. Park and M. G. Kanatzidis, J. Am. Chem. Soc., 111, 3767 (1989). (a) G. Gattow and O. Rosenberg, Z. Anorg. Allg. Chem., 332, 269 (1964). (b) C. Burschka, Z. Naturforsch., 35b, 1511 (1980). Y. Park, Ph.D. Thesis, Michigan State University, East Lansing, MI, 1992. T. M. McCarthy, X. Zhang, and M. G. Kanatzidis, Inorg. Chem., 32, 2944 (1993). (a) C. Burschka, Z. Naturforsch., 34b, 396 (1979). (b) Z. Peplinski, D. B. Brown, T. Watt, W. E. Hatfield, and P. Day, Inorg. Chem., 21, 1752 (1982). (c) M. H. Whangbo and E. Canadell, Inorg. Chem., 29, 1387 (1990). J. C. W. Folmer and F. Jellinek, J. Less-Common Met., 76, 153 (1980). Y. Park, D. C. Degroot, J. Shindler, C. Kannewurf, and M. G. Kanatzidis, Chem. Mater., 5, 8 (1993). R. Berger and L. Eriksson, J. Less-Common Met., 161, 101 (1990). Y. Park, D. C. Degroot, J. Shindler, C. R. Kannewurf, and M. G. Kanatzidis, Angew. Chem. Int. Ed. Engl., 30, 1325 (1991). Y. Park and M. G. Kanatzidis, Chem. Mater., 3, 781 (1991). X. Zhang, J. L. Schindler, T. Hogan, J. Albritton-Thomas, C. R. Kannewurf, and Mercouri G. Kanatzidis, Angew. Chem., 34, 68, (1995). M. G. Kanatzidis, Chem. Mater., 2, 353 (1990). Y. Park and M. G. Kanatzidis, Angew. Chem. Int. Ed. Engl., 29, 914 (1990). C.-N. Chau, W. M. Wardle, and J. A. Ibers, Inorg. Chem., 26, 2740 (1987). D. Fenske, J. Adel, and K. Dehnicke, Z. Naturforsch B, 42, 931 (1987). A. F. Wells, Structural Inorganic Chemistry, Oxford University Press, New York, 1987, p. 414. W. Bronger and O. Gönter, J. Less-Common Met., 27, 73 (1972). E. A. Axtell, Z. Pikramenou, J.-H. Liao, and M. G. Kanatzidis, submitted for publication. E. A. Axtell, J.-H. Liao, Z. Pikramenou, Y. Park, and M. G. Kanatzidis, J. Am. Chem. Soc., 115, 12191 (1993). M. A. Ansari and J. A. Ibers, J. Solid State Chem., 103, 293 (1993). Y. Park and M. G. Kanatzidis, Chem. Mater., 2, 99 (1990). (a) F. G. Donika, G. A. Kiosse, S. I. Radautsan, S. A. Semiletov, and V. F. Zhitar, Sov. Phys. Crystallogr., 12, 745 (1968). (b) R. S. Boorman and J. K. Sutherland, J. Mater. Sci., 4, (8) 658 (1969). (c) D. E. Barnett, R. S. Boorman, and J. K. Sutherland, Phys. Status Solidi A, 4, (1) K49 (1971). K. O. Klepp, J. Alloys Comp., 182, 281 (1992). B. Krebs, S. Pohl, and W. Schiwy, Z. Anorg. Allg. Chemie., 393, 63 (1973). J.-H. Liao, C. Varotsis, and M. G. Kanatzidis, Inorg. Chem., 32, 2453 (1993). K. O. Klepp, Z. Naturforsch., 42b, 197 (1992). G. Z. Eulenberger, Z. Naturforsch., 36b, 687 (1981). A. Müller, Chimia, 39, 25 (1985). R. M. Banda, J. Cusick, M. L. Scudder, D. C. Craig, and I. G. Dance, Polyhedron, 8, 1999 (1985). S. Dhingra, S.-P. Huang, and M. G. Kanatzidis, Polyhedron, 11, 1389 (1990). T. M. McCarthy and M. G. Kanatzidis, Inorg. Chem., 33, 1205 (1994). T. M. McCarthy, T. Tanzer, and M. G. Kanatzidis, J. Am. Chem. Soc., 117, 1294 (1995). T. J. McCarthy, S.-P. Ngeyi, J. H. Liao, D. C. Degroot, T. Hogan, C. R. Kannewurf, and M. G. Kanatzidis, Chem. Mater., 5, 331 (1993). A. S. Kanishcheva, Y. N. Mikhailov, and V. G. Batog, Dokl. Akad. Nauk. SSSR, 251, 603 (1980). Y. V. Vorisholov, E. Y. Peresh, and M. I. Golovei, Inorg. Mater., 8, 677 (1972). P. Villars and L. D. Calvert, Pearson's Handbook of Crystallographic Data for Intermetallic Phases, American Society for Metals, Metals Park, OH, 1985, p. 1494. S. Scavnicar, Z. Kristallogr., 114, 85 (1960). R. S. Mitchel, Z. Kristallogr., 108, 296 (1956). G. Cordier, H. Shafer, and C. Schwidetzky, Rev. Chim. Miner., 22, 676 (1985). G. Cordier, H. Shafer, and C. Schwidetzky, Rev. Chim. Miner., 22, 631 (1985). A. C. Sutorik and M. G. Kanatzidis, manuscript in preparation. A. C. Sutorik and M. G. Kanatzidis, Angew. Chem. Int. Ed., Engl., 31, 1594 (1992). A. C. Sutorik and M. G. Kanatzidis, J. Am. Chem. Soc., 113, 7754 (1991). A. C. Sutorik and M. G. Kanatzidis, manuscript in preparation. W. Kroniert and K. Plieth, Z. Anorg. Allg. Chem., 336, 207 (1965). P. M. Keane and J. A. Ibers, J. Solid State Chem., 93, 291 (1991). A. C. Sutorik and M. G. Kanatzidis, J. Am. Chem. Soc., 116, 7706 (1994). A. C. Sutorik and M. G. Kanatzidis, to be published. (a) D. Coucouvanis, Acc. Chem. Res., 14, 201 (1981). (b) R. H. Holm, Chem. Soc. Rev., 10, 455 (1981). (c) A. Müller, E. Diemann, R. Jostes, and H. Bögge, Angew. Chem., Int. Ed., Engl., 20, 934 (1981). W. P. Binnie, M. J. Redman, and W. Mallio, Inorg. Chem., 9, 1449 (1970). E. A. Pruss and A. M. Stacy, 203rd ACS National Meeting 1992, Washington DC. J.-H. Liao and M. G. Kanatzidis, Chem. Mater., 5, 1561 (1993). G. K. Averkieva, A. A. Vaipolin, and N. A. Goryunova, in Some Ternary Compounds of the A2(I)B(IV)C3(VI) Type and Solid Solutions Based on Them, Soviet Research in New Semiconductor Materials, D. N. Nasledov, Ed., Consultants Bureau, New York, 1965, pp. 26– 34. (a) W. Bronger and P. Böttcher, Z. Anorg. Alleg. Chem., 390, 1 (1972). (b) W. Bronger and U. Hendriks, Rev. Chim. Miner., 17, 555 (1980). (c) W. Bronger and P. Müller, J. Less-Common Met., 100, 241 (1984). J.-H. Liao, Ph.D. Thesis, Michigan State University, East Lansing, MI, 1993. W. Schiwy, Chr. Blutau, D. Gäthje, and B. Krebs, Z. Anorg. Allg. Chem., 412, 1 (1975). (a) H. Hahn and W. Klingen, Naturwissenschaften, 52, 494 (1965). (b) H. Hahn, R. Ott, and W. Klingen, Z. Anorg. Allg. Chem., 396, 271 (1973). (a) R. Diehl and C.-D. Carpentier, Acta Crystallogr. Ser. B, 34, 1097 (1978). (b) P. Buck and C.-D. Carpentier, Acta Crystallogr. Ser. B, 29, 1864 (1973). (c) H. Zimmerman, C.-D. Carpentier, and R. Nitsche, Acta Crystallogr. Ser. B, 31, 2003 (1975). (d) R. Becker, W. Brockner, and B. Eisenmann, Z. Naturforsch., 42a, 1309 (1987). (e) A. Ferrari and L. Cavalca, Gazz. Chim. Ital. 78, 283 (1948). (f) R. Diehl and C.-D. Carpentier, Acta Crystallogr. Ser. B, 33, 1399 (1977). (g) A. Simon, K. Peters, E.-M. Peters, and H. Hahn, Z. Naturforsch., 38b, 426 (1983). (h) M. Jansen and U. Henseler, J. Solid State Chem., 99, 110 (1992). (a) P. Toffoli, J. C. Rouland, P. Khodadad, and N. Rodier, Acta Crystallogr. Ser. C, 41, 645 (1985). (b) P. Toffoli, P. Khodadad, and N. Rodier, Acta Crystallogr. Ser. B, 38, 2374 (1982). (c) P. Toffoli, P. Khodadad, and N. Rodier, Bull. Soc. Chim. Fr., 11, 429 (1981). (a) R. Mercier, J.-P. Malugani, B. Fahys, and G. Robert, Acta Crystallogr. Ser. B, 38, 1887 (1982). (b) S. Fiechter, W. F. Kuhs, and R. Nitsche, Acta Crystallogr., Ser. B, 36, 2217 (1980). (c) H. Schafer, G. Schafer, and A. Weiss, Z. Naturforsch., 20b, 811 (1965). (d) R. Brec, M. Evain, P. Grenouilleau, and J. Rouxel, Rev. Chim. Min., 20, 283 (1983). (e) R. Brec, M. Evain, P. Grenouilleau, and J. Rouxel, Rev. Chim. Min., 20, 283 (1983). (e) R. Brec, P. Grenouilleau, M. Evain, and J. Rouxel, Rev. Chim. Min., 20, 295 (1983). (f) M. Evain, S. Lee, M. Queignec, and R. Brec, J. Solid State Chem., 71, 139 (1987). (g) M. Z. Jandali, G. Eulenberger, and H. Hahn, Z. Anorg. Allg. Chem., 530, 144 (1985). (h) A. Weiss and H. Schafer, Z. Naturforsch, 18b, 81 (1963). F. Menzel, L. Ohse, and W. Brockner, Heteroatom. Chem., 1, (5) 357 (1990). T. M. McCarthy and M. G. Kanatzidis, Chem. Mater., 5, 1061 (1993). E. Durand, M. Evain, and R. Brec, J. Solid State Chem., 102, 146 (1992). P. Toffoli, P. Khodadad, and N. Rodier, Acta Crystallogr. Ser. B, 33, 1492 (1977). M. Z. Jandali, G. Eulenberger, and H. Hahn, Z. Anorg. Allg. Chem., 445, 184 (1978). W. Honle, C. Wibbelmann, and W. Brockner, Z. Naturforusch., 39b, 1088 (1984). (a) T. M. McCarthy, Ph.D. Thesis, (b) T. McCarthy and M. G. Kanatzidis, submitted for publication. (c) Timothy J. McCarthy and Mercouri G. Kanatzidis, Inorg. Chem., 34, 1257 (1995). (d) T. J. McCarthy, T. Hogan, C. R. Kannewurf, and M. G. Kanatzidis, Chem. Mater., 6, 1072 (1994). T. M. McCarthy and M. G. Kanatzidis, unpublished results. C. L. Teske, Z. Naturforsch., 34B, 544 (1979). T. M. McCarthy and M. G. Kanatzidis, J. Chem. Soc. Chem. Commun., 1089 (1994). X. Zhang and M. G. Kanatzidis, J. Am. Chem. Soc., 116, 1890 (1994). X. Zhang and M. G. Kanatzidis, Inorg. Chem., 33, 1238 (1994). A. F. Wells, Structural Inorganic Chemistry, 5th ed., Clarendon Press, Oxford, UK, 1984, pp. 258– 260. L. Gmelin, Handbuch der Anorganischen Chemie, Springer-Verlag, Berlin, System, Number 56, Teil C6, 1976, pp. 77– 78. D. Coucouvanis, P. B. Patil, M. G. Kanatzidis, B. Detering, and N. C. Baenziger, Inorg. Chem., 24, 24 (1985). A. Müller, M. Zimmerman, and H. Bögge, Angew. Chem. Int. Ed. Engl., 25, 273 (1986). A. Müller, J. Schimanski, and U. Schimanski, Angew. Chem. Int. Ed. Engl., 23, 159 (1984). S. Dhingra and M. G. Kanatzidis, Polyhedron, 10, 1069 (1991). (a) J. M. Charnock, C. D. Garner, R. A. Pattrick, and D. J. Vaughan, J. Solid State Chem., 82, 279 (1989). (b) B. J. Wuensch, Z. Kristallogr., 119, 437 (1964). (c) L. Pauling and E. W. Newmann, Z. Kristallogr., 88, 54 (1934). (a) W. Rüdorff, H. G. Scharz, and M. Walter, Z. Anorg. Allg. Chem., 269, 141 (1952). (b) D. B. Brown, J. A. Zubieta, P. A. Vella, T. Wrobleski, T. Watt, W. E. Hatfield, and P. Day, Inorg. Chem., 19, 1945 (1980). (c) K. O. Klepp, H. Boller, and H. Völlenkle, Monatsh. Chem., 111, 727 (1980). C. Burschka, Z. Anorg. Allg. Chem., 463, 65 (1980). (a) C. Burschka, Z. Naturforsch., 34b, 675 (1979). (b) L. W. Huar, F. J. DiSalvo, H. E. Bair, R. M. Fleming, J. V. Waszczak, and W. E. Hatfield, Phys. Rev. B, 35, (4) 1932 (1987). (c) R. M. Flemming, L. W. Haar, and F. J. DiSalvo, Phys. Rev. B, 35, (10) 5388 (1987). G. J. Janz, E. Roduner, J. W. Coutts, and J. R. Downey, Jr., Inorg. Chem., 15, (8) 1751 (1976). S. Dhingra and M. G. Kanatzidis, Science, 258, 1769 (1992). D. Chakrabarty and M. G. Kanatzidis, to be published. J. Fortner, M.-L. Saboungi, and J. E. Enderby, Phys. Rev. Lett. 69, 1415 (1992). For another recent review, see J. A. Cody, M. F. Mansuetto, S. Chien, and J. A. Ibers, Mat. Sci. Forum, 152–153, 35 (1994). Progress in Inorganic Chemistry, Volume 43 ReferencesRelatedInformation
Referência(s)