Artigo Acesso aberto Revisado por pares

Using cavity ringdown spectroscopy for continuous monitoring of δ 13 C(CO 2 ) and ƒCO 2 in the surface ocean

2012; Wiley; Volume: 10; Issue: 10 Linguagem: Inglês

10.4319/lom.2012.10.752

ISSN

1541-5856

Autores

Meike Becker, Nils Andersen, Björn Fiedler, Peer Fietzek, Arne Körtzinger, Tobias Steinhoff, Gernot Friedrichs,

Tópico(s)

Atmospheric and Environmental Gas Dynamics

Resumo

The role of the global surface ocean as a source and sink for atmospheric carbon dioxide and the flux strengths between the ocean and the atmosphere can be quantified by measuring the fugacity of CO 2 (ƒCO 2 ) as well as the dissolved inorganic carbon (DIC) concentration and its isotopic composition in surface seawater. In this work, the potential of continuous wave cavity ringdown spectroscopy ( cw ‐CRDS) for autonomous underway measurements of ƒCO 2 and the stable carbon isotope ratio of DIC [δ 13 C(DIC)] is explored. For the first time, by using a conventional air‐sea equilibrator setup, both quantities were continuously and simultaneously recorded during a field deployment on two research cruises following meridional transects across the Atlantic Ocean (Bremerhaven, Germany—Punta Arenas, Chile). Data are compared against reference measurements by an established underway CO 2 monitoring system and isotope ratio mass spectrometric analysis of individual water samples. Agreement within ΔƒCO 2 = 0.35 µatm for atmospheric and ΔƒCO 2 = 2.5 µatm and Δδ 13 C(DIC) = 0.33‰ for seawater measurements have been achieved. Whereas “calibration‐free” ƒCO 2 monitoring is feasible, the measurement of accurate isotope ratios relies on running reference standards on a daily basis. Overall, the installed CRDS/equilibrator system was shown to be capable of reliable online monitoring of ƒCO 2 , equilibrium δ 13 C(CO 2 ), δ 13 C(DIC), and p O 2 aboard moving research vessels, thus making possible corresponding measurements with high spatial and temporal resolution.

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