Synthesis of N,N ‐Bis(dialkoxyphosphinoylmethyl)‐ and N,N ‐Bis(diphenylphosphinoylmethyl)‐β‐ and γ‐amino acid Derivatives by the Microwave‐Assisted Double Kabachnik

Artigo Revisado por pares

Synthesis of N,N ‐Bis(dialkoxyphosphinoylmethyl)‐ and N,N ‐Bis(diphenylphosphinoylmethyl)‐β‐ and γ‐amino acid Derivatives by the Microwave‐Assisted Double Kabachnik–Fields Reaction

2014; Wiley; Volume: 26; Issue: 1 Linguagem: Inglês

10.1002/hc.21221

ISSN

1098-1071

Autores

Erika Bálint, Eszter Fazekas, János Kóti, György Keglevich,

Tópico(s)

Synthesis and Reactivity of Sulfur-Containing Compounds

Resumo

ABSTRACT The title compounds were synthesized by the microwave‐assisted, mostly solvent‐free bis Kabachnik–Fields condensation of β‐alanine and γ‐aminobutyric acid or their esters with formaldehyde and >P(O)H species, such as dialkyl phosphites and diphenylphosphine oxide.

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Synthesis of N,N ‐Bis(dialkoxyphosphinoylmethyl)‐ and N,N ‐Bis(diphenylphosphinoylmethyl)‐β‐ and γ‐amino acid Derivatives by the Microwave‐Assisted Double Kabachnik–Fields Reaction