Produção Nacional
Revisado por pares
Extração e isolamento de alfa-solanina de brotos de batata
1983; INSTITUTO AGRONÔMICO DE CAMPINAS; Volume: 42; Issue: 1 Linguagem: Inglês
10.1590/s0006-87051983000100025
ISSN1678-4499
AutoresDayse Soave Spoladore, Marco Antônio Teixeira Zullo, João Paulo Feijão Teixeira,
Tópico(s)Potato Plant Research
ResumoFresh potato sprouts were extracted with 2% aqueous acetic acid for 48 hours. The crude alkaloidal extract was purified by repeating the operation. Precipitation by concentrated ammonium hydroxide, centrifugation, dissolution of the resulting precipitate in 2% acetic acid, till a clear alkaline supernatant was obtained. The a-solanine, obtained by this procedure was purified by successive recristalizations with ethyl alcohol. The total yield was about 0.02% of the fresh material, with purity greater than 99%. IR, 1H and 13C NMR spectra are shown.
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