The Analysis of Putrescine in Plant Samples by Automated Hplc

1981; Marcel Dekker; Volume: 4; Issue: 7 Linguagem: Inglês

10.1080/01483918108068811

ISSN

2331-0413

Autores

Denis R. Lauren, Connie Parker, Michael Agnew, GH Smith,

Tópico(s)

Mycotoxins in Agriculture and Food

Resumo

Abstract The quantitative analysis of putrescine from plant tissue can be achieved using isocratic reversed-phase high performance liquid chromatography (HPLC). After preliminary extraction and clean up involving an ion exchange purification step, the isolated diamines are derivatised with benzoyl chloride for determination by HPLC. Automation of the HPLC step has led to a considerable saving in time for the total analysis. Potential problems associated with the analytical procedure are described.

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