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Slurry Sampling—An Analytical Strategy for the Determination of Metals and Metalloids by Spectroanalytical Techniques

2010; Taylor & Francis; Volume: 45; Issue: 1 Linguagem: Inglês

10.1080/05704920903435474

1520-569X

Sérgio L.C. Ferreira, Manuel Miró, Erik Galvão Paranhos da Silva, Geraldo D. Matos, Pedro Sanches dos Reis, Geovani C. Brandão, Walter Nei Lopes dos Santos, Álvaro T. Duarte, Maria Goreti Rodrigues Vale, Rennan G.O. Araújo,

Mercury impact and mitigation studies

Abstract This article critically overviews the state-of-the-art of slurry sampling as an approach for the minimization of sample preparation prior to the determination of metals and metalloids in complex matrices by spectroanalytical techniques. Relevant factors involved in the optimization of slurry-based analytical procedures and the dependence of the quality of the results on the calibration method selected are discussed in detail. The advantages and limitations compared to solid sampling for the analysis of solid matrices are highlighted and discussed. Analytical applications of slurry sampling reported in the literature emphasizing publications between 2004 and 2009 are comprehensively compiled covering detection by flame atomic absorption spectrometry (FAAS), electrothermal atomic absorption spectrometry (ET-AAS), cold vapor atomic absorption spectrometry (CV-AAS), hydride generation atomic absorption spectrometry (HG-AAS), hydride generation atomic fluorescence spectrometry (HG-AFS), inductively coupled plasma optical emission spectrometry (ICP-OES), and inductively coupled plasma mass spectrometry (ICP-MS).