Voltar
Artigo Revisado por pares
BIBTEX RIS

One-Pot Synthesis of New-Phase AgInSe 2 Nanorods

2006; American Chemical Society; Volume: 128; Issue: 22 Linguagem: Inglês

10.1021/ja060543u

ISSN

1943-2984

Autores

Meng T. Ng, Chris Boothroyd, Jagadese J. Vittal,

Tópico(s)

Copper-based nanomaterials and applications

Resumo

AgInSe2 nanorods with a previously unknown orthorhombic phase isostructural to AgInS2 have been prepared by the thermolysis of [(PPh3)2AgIn(SeC{O}Ph)4] in a mixture of oleylamine (OA) and dodecanethiol (DT) at 185 degrees C. A systematic study indicates that the ratio of surfactants is crucial for obtaining both monodispersed nanorods and the new orthorhombic phase AgInSe2. The AgInSe2 nanorods have been characterized by TEM, XRPD, EDX, and XPS.

Referência(s)