
Determinação simultânea de trialometanos e agrotóxicos em água por cromatografia gasosa
2011; Brazilian Chemical Society; Volume: 34; Issue: 2 Linguagem: Inglês
10.1590/s0100-40422011000200019
ISSN1678-7064
AutoresElenice A. Carlos, Antônio Augusto Neves, César Reis, José Humberto de Queiróz,
Tópico(s)Environmental Chemistry and Analysis
ResumoBY GAS CHROMATOGRAPHY.A method for simultaneous analysis of trihalomethanes and organochloride and pyrethroid pesticides in water utilizing SPME-HS and GC-ECD was developed.In the optimized method 25 mL of water containing 2% (w/v) Na 2 HPO 4 were heated to 60 °C for 50 min.The fiber (PDMS -100 mm) was exposed to a headspace for the same period.For all analytes it was found that LOQ < MCL (Maximum Contaminant Level), CV < 20% and r > 0.9.The method was applied to potable and surface water samples.Some trihalomethanes were encountered in potable waters, at levels below the MCL.
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