The crystal and molecular structure of an unusual 49 heterocycle, 62 2‐thia‐1,3,5‐triaza‐7‐phosphaadamantane 2,2‐dioxide 51
1976; Wiley; Volume: 13; Issue: 4 Linguagem: Inglês
10.1002/jhet.5570130414
ISSN1943-5193
AutoresJ. R. DELERNO, L. M. Trefonas, R. J. Majeste,
Tópico(s)Organometallic Complex Synthesis and Catalysis
ResumoAbstract The crystal and molecular structure of 2‐thia‐1,3,5‐triaza‐7‐phosphaadamantane 2,2‐dioxide (C 5 H 10 SPO 2 N 3 ) has been determined by single crystal x‐ray diffraction techniques. The compound crystallizes in the space group P2 1 /c with four formula weights per unit cell of dimensions a = 6.129 (1) Å, b = 12.440 (2) Å, c = 14.028 (2) Å, β = 127.31 (1)°. The structure was solved by direct methods and refined to a final value of R = 0.079.
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