In-situ X-ray diffraction of palladium cathodes in electrolytic cells
1989; Elsevier BV; Volume: 71; Issue: 10 Linguagem: Inglês
10.1016/0038-1098(89)90201-9
ISSN1879-2766
AutoresE. Batalla, E. G. Zwartz, B. A. Judd,
Tópico(s)X-ray Diffraction in Crystallography
ResumoX-ray diffraction spectra of palladium electrodes have been measured while being charged with hydrogen or deuterium in an electrolysis cell. Changes in the lattice parameter have been recorded as a function of electrolysis time, showing a transition from the low hydrogen α phase to the ß phase, PdH. No further structural transition beyond this phase has been observed.
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