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NMR Spectroscopy of Laser‐Polarized 129 Xe Under Continuous Flow: A Method To Study Aqueous Solutions of Biomolecules

2006; Wiley; Volume: 45; Issue: 43 Linguagem: Inglês

10.1002/anie.200601008

1521-3773

Daniela Baumer, Eike Brunner, Peter Blümler, Paul P. Zänker, H. W. Spieß,

Advanced NMR Techniques and Applications

Angewandte Chemie International EditionVolume 45, Issue 43 p. 7282-7284 Communication NMR Spectroscopy of Laser-Polarized 129Xe Under Continuous Flow: A Method To Study Aqueous Solutions of Biomolecules† Daniela Baumer Dr., Daniela Baumer Dr. Institut für Biophysik und Physikalische Biochemie, Universität Regensburg, Universitätsstrasse 31, 93040 Regensburg, Germany, Fax: (+49) 941-943-2479Search for more papers by this authorEike Brunner Prof., Eike Brunner Prof. eike.brunner@biologie.uni-regensburg.de Institut für Biophysik und Physikalische Biochemie, Universität Regensburg, Universitätsstrasse 31, 93040 Regensburg, Germany, Fax: (+49) 941-943-2479Search for more papers by this authorPeter Blümler Dr., Peter Blümler Dr. Max-Planck-Institut für Polymerforschung, Ackermannweg 10, 55128 Mainz, Germany, Fax: (+49) 6131-379-100 Research Center Jülich, ICG III, 52425 Jülich, GermanySearch for more papers by this authorPaul Philipp Zänker Dipl.-Phys., Paul Philipp Zänker Dipl.-Phys. Max-Planck-Institut für Polymerforschung, Ackermannweg 10, 55128 Mainz, Germany, Fax: (+49) 6131-379-100Search for more papers by this authorHans Wolfgang Spiess Prof., Hans Wolfgang Spiess Prof. spiess@mpip-mainz.mpg.de Max-Planck-Institut für Polymerforschung, Ackermannweg 10, 55128 Mainz, Germany, Fax: (+49) 6131-379-100Search for more papers by this author Daniela Baumer Dr., Daniela Baumer Dr. Institut für Biophysik und Physikalische Biochemie, Universität Regensburg, Universitätsstrasse 31, 93040 Regensburg, Germany, Fax: (+49) 941-943-2479Search for more papers by this authorEike Brunner Prof., Eike Brunner Prof. eike.brunner@biologie.uni-regensburg.de Institut für Biophysik und Physikalische Biochemie, Universität Regensburg, Universitätsstrasse 31, 93040 Regensburg, Germany, Fax: (+49) 941-943-2479Search for more papers by this authorPeter Blümler Dr., Peter Blümler Dr. Max-Planck-Institut für Polymerforschung, Ackermannweg 10, 55128 Mainz, Germany, Fax: (+49) 6131-379-100 Research Center Jülich, ICG III, 52425 Jülich, GermanySearch for more papers by this authorPaul Philipp Zänker Dipl.-Phys., Paul Philipp Zänker Dipl.-Phys. Max-Planck-Institut für Polymerforschung, Ackermannweg 10, 55128 Mainz, Germany, Fax: (+49) 6131-379-100Search for more papers by this authorHans Wolfgang Spiess Prof., Hans Wolfgang Spiess Prof. spiess@mpip-mainz.mpg.de Max-Planck-Institut für Polymerforschung, Ackermannweg 10, 55128 Mainz, Germany, Fax: (+49) 6131-379-100Search for more papers by this author First published: 30 October 2006 https://doi.org/10.1002/anie.200601008Citations: 35 † We thank S. Appelt and W. Häsing (FZ Jülich) for the development of the xenon polarizer and H.-D. Lemke (Membrana GmbH) for the oxygenator fiber membranes. Financial support from the DFG (Br 1278/12-1 and Sp 98/6-2) is gratefully acknowledged. Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinked InRedditWechat Abstract Go with the flow: In many applications of NMR spectroscopy in chemistry, proper sample preparation is absolutely critical for success, in particular in biochemical and biomedical areas. For the NMR spectroscopy of laser-polarized 129Xe, an efficient and robust method for continuous flow of the gas to a NMR tube was developed. Applications to H2O, DMSO, phospholipid bicelles, and 2D exchange NMR spectroscopy are demonstrated. Citing Literature Supporting Information Supporting information for this article is available on the WWW under http://www.wiley-vch.de/contents/jc_2002/2006/z601008_s.pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. Volume45, Issue43November 6, 2006Pages 7282-7284 RelatedInformation