Artigo Revisado por pares

The first synthesis of peptide thioester carrying N-linked core pentasaccharide through modified Fmoc thioester preparation: synthesis of an N-glycosylated Ig domain of emmprin

2003; Elsevier BV; Volume: 44; Issue: 14 Linguagem: Inglês

10.1016/s0040-4039(03)00394-0

ISSN

1873-3581

Autores

Hironobu Hojo, Eiichiro Haginoya, Yoshiyuki Matsumoto, Yoshiaki Nakahara, Kazuki Nabeshima, Bryan P. Toole, Yasushi Watanabe,

Tópico(s)

Biochemical and Structural Characterization

Resumo

Peptide thioester carrying N-linked core pentasaccharide was prepared by the Fmoc solid-phase method with a combination of the benzyl-protection strategy at the carbohydrate portion. The obtained peptide thioester was successfully used for the synthesis of the first Ig domain of emmprin composed of 61 amino acid residues.

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