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Fused s ‐triazino heterocycles. I. s ‐triazino[2,1‐ b ]quinazolinones and s ‐triazino[1,2‐ c ]quinazolinone

1972; Wiley; Volume: 9; Issue: 1 Linguagem: Italiano

10.1002/jhet.5570090122

1943-5193

John T. Shaw, D. Taylor, Franklin J. Corbett, John D. Ballentine,

Synthesis and Reactivity of Heterocycles

Journal of Heterocyclic ChemistryVolume 9, Issue 1 p. 125-130 Note Fused s-triazino heterocycles. I. s-triazino[2,1-b]quinazolinones and s-triazino[1,2-c]quinazolinone† John T. Shaw, John T. Shaw Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this authorDiane M. Taylor, Diane M. Taylor Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this authorFranklin J. Corbett, Franklin J. Corbett Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this authorJohn D. Ballentine, John D. Ballentine Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this author John T. Shaw, John T. Shaw Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this authorDiane M. Taylor, Diane M. Taylor Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this authorFranklin J. Corbett, Franklin J. Corbett Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this authorJohn D. Ballentine, John D. Ballentine Department of Chemistry, Grove City College, Grove City, Pennsylvania 16127Search for more papers by this author First published: February 1972 https://doi.org/10.1002/jhet.5570090122Citations: 8 † Taken in part from the Senior Honors Projects of Diane M. Taylor, 1970, Franklin J. Corbett, 1970, and John D. Ballentine, 1969. AboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL References 2 J. T. Shaw and J. Ballentine, Chem. Commun., 1040, (1969). 3 An alternate structure, 4-phenyl-2,6-diimino-2,6-dihydro-11-H-s-triazino[2,1-b]quinazoline hydrochloride, is also possible by this synthesis. 4a H. K. Reimschuessel and N. T. McDevitt, J. Am. Chem. Soc., 82, 3760 (1960). (b) W. Pearlman and C. Banks, J. Am. Chem. Soc., 70, 3726 (1948). (c) J. T. Thurston, J. R. Dudley, D. W. Kaiser, I. Hechenbleikner, F. C. Schaefer and D. Holm-Hansen, J. Am. Chem. Soc., 73, 2983, (1951). (d) F. H. S. Curd, J. K. Landquist and F. L. Rose, J. Chem. Soc., 154 (1947). 5 2-Chloro-4,6-bis(benzylamino)-s-triazine, m.p. 240–241°, was prepared using method of Thurston et al. (4c), Anal. Calcd. For C17H16ClN5: C, 62.7; H, 4.94; N, 21.5. Found: C, 62.7; H, 4.90; N, 21.4. 6 F. H. S. Curd, J. K. Landquist and F. L. Rose, J. Chem. Soc., 755 (1947). 7 J. T. Shaw, J. Org. Chem., 27, 3890 (1962). 8 J. T. Shaw, U. S. Patent No. 3,215,693 (1965) Chem. Abstr., 64, 2110 (1966). 9 This experiment was mentioned in a previous communication (2) but no experimental details were given. 10 K. R. Huffman and F. C. Schaefer, J. Org. Chem., 28, 1812 (1963). 11 J. T. Shaw and R. Adams, J. Chem. Eng. Data, 13, 142 (1968). 12 H. C. Scarborough, B. C. Lawes, J. L. Minielli and J. L. Compton, J. Org. Chem., 27, 957 (1962). Citing Literature Volume9, Issue1February 1972Pages 125-130 ReferencesRelatedInformation