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Improved Procedure for the Oxidative Cleavage of Olefins by OsO 4 −NaIO 4

2004; American Chemical Society; Volume: 6; Issue: 19 Linguagem: Inglês

10.1021/ol0400342

1523-7060

Wensheng Yu, Yan Mei, Ying Kang, Zhengmao Hua, Zhendong Jin,

Catalytic C–H Functionalization Methods

Oxidative cleavage of olefins by OsO4−NaIO4 sometimes suffers from low yields due to the formation of side products. It is found that the addition of 2,6-lutidine can suppress the side reactions and dramatically improve the yield of this classic reaction.