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Artigo Revisado por pares
BIBTEX RIS

A mild method for rapid tert-butyldiphenylsilylation of primary and secondary alcohols

1993; Elsevier BV; Volume: 34; Issue: 24 Linguagem: Inglês

10.1016/s0040-4039(00)79237-9

ISSN

1873-3581

Autores

Steven A. Hardinger, Ngadi Wijaya,

Tópico(s)

Chemical Synthesis and Analysis

Resumo

A rapid and efficient method for the protection of primary and secondary alcohols as their tert-butyldiphenylsilyl (tBDPS) ethers was developed. Reaction of the alcohol and tBDPSCl in DMF with AgNO3, NH4NO3, or NH4ClO4 provides good yields of the corresponding silyl ethers

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