XRD, SEM-EDS, and FTIR studies ofin vitro growth of an apatite-like layer on sol-gel glasses

1999; Wiley; Volume: 44; Issue: 4 Linguagem: Inglês

10.1002/(sici)1097-4636(19990315)44

ISSN

1097-4636

Autores

M. Vallet-Reg�, Ana Romero, C. V. Ragel, Racquel Z. LeGeros,

Tópico(s)

Facial Trauma and Fracture Management

Resumo

Journal of Biomedical Materials ResearchVolume 44, Issue 4 p. 416-421 XRD, SEM-EDS, and FTIR studies of in vitro growth of an apatite-like layer on sol-gel glasses M. Vallet-Regí, Corresponding Author M. Vallet-Regí [email protected] Departamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainDepartamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainSearch for more papers by this authorA. M. Romero, A. M. Romero Departamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainSearch for more papers by this authorC. V. Ragel, C. V. Ragel Departamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainSearch for more papers by this authorR. Z. LeGeros, R. Z. LeGeros New York University College of Dentistry, 345 East 24th Street, New York, New York 10010Search for more papers by this author M. Vallet-Regí, Corresponding Author M. Vallet-Regí [email protected] Departamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainDepartamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainSearch for more papers by this authorA. M. Romero, A. M. Romero Departamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainSearch for more papers by this authorC. V. Ragel, C. V. Ragel Departamento de Química Inorgánica y Bioinorgánica, Facultad de Farmacia, UCM E-28040, Madrid, SpainSearch for more papers by this authorR. Z. LeGeros, R. Z. LeGeros New York University College of Dentistry, 345 East 24th Street, New York, New York 10010Search for more papers by this author First published: 29 January 1999 https://doi.org/10.1002/(SICI)1097-4636(19990315)44:4 3.0.CO;2-SCitations: 152AboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Abstract A glass with a composition (in mole %) of: SiO2 (70), CaO (26), and P2O5 (4) was obtained using a sol-gel method. The in vitro bioactivity of the glass was assessed by determining the changes in surface morphology and composition after soaking in simulated body fluid (SBF) for periods of up to 14 days at 37°C. X-ray diffraction, scanning electron microscopy, X-ray energy dispersive spectroscopy, and FTIR analyses of the glass surface after different soaking periods in SBF demonstrated the growth of an apatite-like layer on the glass surface. In the first stage, an amorphous calcium phosphate layer was formed; after 7 days this surface consisted of spheres, with diameters ranging between 2 and 15 μm, composed of needle-like apatite crystallites (250 × 100 nm) with a crystallinity similar to that of a biological apatite. © 1999 John Wiley & Sons, Inc. J Biomed Mater Res, 44, 416–421, 1999. Citing Literature Volume44, Issue415 March 1999Pages 416-421 RelatedInformation

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