Artigo Acesso aberto

Crystal Structure of the OXA-48 β-Lactamase Reveals Mechanistic Diversity among Class D Carbapenemases

2009; Elsevier BV; Volume: 16; Issue: 5 Linguagem: Inglês

10.1016/j.chembiol.2009.04.010

ISSN

1879-1301

Autores

Jean‐Denis Docquier, V. Calderone, Filomena De Luca, Manuela Benvenuti, Francesco Giuliani, Luca Bellucci, Andrea Tafi, Patrice Nordmann, Maurizio Botta, Gian María Rossolini, Stefano Mangani,

Tópico(s)

Bacterial Genetics and Biotechnology

Resumo

Carbapenem-hydrolyzing class D beta-lactamases (CHDLs) are enzymes found in important Gram-negative pathogens (mainly Acinetobacter baumannii and Enterobacteriaceae) that confer resistance to beta-lactam antibiotics, and notably carbapenems. The crystal structure of the OXA-48 carbapenemase was determined at pH 7.5 and at a resolution of 1.9 A. Surprisingly, and by contrast with OXA-24, the only other CHDL of known crystal structure, the structure of OXA-48 was similar to OXA-10, an enzyme devoid of carbapenemase activity, indicating that the hydrolysis of these compounds could depend on subtle changes in the active site region. Moreover, the active site groove of OXA-48 was different from that of OXA-24 in shape, dimensions, and charge distribution. Molecular dynamics pointed to the functional relevance of residues located in or close to the beta5-beta6 loop and allowed us to propose a mechanism for carbapenem hydrolysis by OXA-48.

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