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BIBTEX RIS

Crystal structure of bis(benzylammonium) lead tetrachloride, (C7H7NH3)2PbCl4

1999; De Gruyter; Volume: 214; Issue: 3 Linguagem: Inglês

10.1515/ncrs-1999-0318

ISSN

2197-4578

Autores

M. Braun, Wolfgang Frey,

Tópico(s)

Solid-state spectroscopy and crystallography

Resumo

Ci4H 2 oCl 4 N2Pb, orthorhombic, Cmc2\ (No. 36), a =33.619(7)Â, b =7.820(l)Ä,c =7.728(1) A, V=2031.6 Â 3 , Z= 4, R gí (F) = 0.021, R W (F 2 ) = 0.054, Τ = 293 Κ. Source of materialThe colorless crystals were grown from solution of lead chloride and benzylammonium chloride (1:2) in dimethylformamide by slowly evaporation of the solvent.Benzylamine was obtained from Merck.The adjunct chloride salt was prepared by addition of a stoichiometric amount of 37% concentrated HCl.

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