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An Efficient Method for the Preparation of Pure Long-Chain CIS-and Trans-2-n-Alkyl-5-Hydroxy-1,3-Dioxanes #

1996; Taylor & Francis; Volume: 26; Issue: 22 Linguagem: Inglês

10.1080/00397919608004651

1532-2432

Andrzej Piasecki, Bogdan Burczyk, Adam Sokołowski, Urszula Kotlewska,

Analytical Chemistry and Chromatography

Abstract The title compounds were obtained with high yields from four-component mixtures of glycerol acetals by combining the transacetalization reaction with the crystallization process followed by fractional distillation. Part XXII in the series: Acetals and Ethers. For Part XXI see Ref. 1 Notes Part XXII in the series: Acetals and Ethers. For Part XXI see Ref. 1