Artigo Revisado por pares

Improving the electrical conductivity of polymer acid-doped polyaniline by controlling the template molecular weight

2007; Royal Society of Chemistry; Volume: 17; Issue: 13 Linguagem: Inglês

10.1039/b618521e

ISSN

1364-5501

Autores

Joung Eun Yoo, Jennifer L. Cross, Tracy L. Bucholz, Kwang Seok Lee, Matthew P. Espe, Yueh‐Lin Loo,

Tópico(s)

Advanced Sensor and Energy Harvesting Materials

Resumo

We report the synthesis and characterization of a series of polyanilines (PANI) that are templated with a polymer acid at varying molecular weights. The polymer acid template of choice, poly(2-acrylamido-2-methyl-1-propanesulfonic acid), or PAAMPSA, was synthesized via conventional free-radical polymerization with molecular weights ranging from 45 kg mol−1 to 724 kg mol−1. Subsequent aniline polymerization in the presence of PAAMPSA yielded water-dispersible, conductive PANI–PAAMPSA. The electrical conductivity of PANI–PAAMPSA increases by approximately three-fold with decreasing PAAMPSA molecular weight. This trend is accompanied by significant structural changes, including increases in PANI crystallinity and conjugation length. These conductivities (0.4–1.1 S cm−1) exceed the highest reported for polymer acid-doped PANI systems.

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