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Expedient Synthesis of t -Butyl Azide

1997; Taylor & Francis; Volume: 27; Issue: 8 Linguagem: Inglês

10.1080/00397919708006078

1532-2432

Jeffrey C. Bottaro, Paul E. Penwell, Robert J. Schmitt,

Machine Learning in Materials Science

Abstract Abstract A simple, economical synthesis of bulk (1 to 10,000 moles) quantities of t-butyl azide is described, utilizing only t-butyl alcohol, water, sodium azide, and sulfuric acid.