Portal de Periódicos da CAPES

Synthesis of LaAlO3 powder using triethanolamine

2007; Elsevier BV; Volume: 34; Issue: 2 Linguagem: Inglês

10.1016/j.ceramint.2006.10.012

1873-3956

Songlin Ran, Lian Gao,

Catalysis and Oxidation Reactions

LaAlO3 powders were successfully synthesized by pyrolysis of complex compounds of lanthanum and aluminum with triethanolamine (TEA). The precursors and the derived powders were characterized by simultaneous thermogravimetry analysis (TG) and differential scanning calorimetry analysis (DSC), X-ray diffractometry (XRD), specific surface area measurements, and transmission electron microscopy (TEM). Pure LaAlO3 phase was obtained at 775 °C for 2 h or 750 °C for 4 h, without formation of any intermediate phase. Pores were found from TEM images of LaAlO3 powders prepared at 800 °C for 2 h.