Artigo Revisado por pares

Confocal μ-XRF depth analysis of paint layers

2004; Elsevier BV; Volume: 219-220; Linguagem: Inglês

10.1016/j.nimb.2004.01.024

ISSN

1872-9584

Autores

Ž. Šmit, Koen Janssens, K. Proost, I. Langus,

Tópico(s)

Nuclear Physics and Applications

Resumo

Focused narrow-band beam of the synchrotron radiation was used for in-depth analysis of historic and modern paint layers. The fluorescent radiation induced by 21 keV impact radiation was detected by a Si(Li) detector equipped with a polycapillary X-ray lens in con-focal geometry. Scanning of the sample was performed by a motorized x–y–z stage. Space resolution of 30 μm was achieved. The procedure of evaluation of concentrations was based on the independent parameter method and included absorption of radiation in the outer layers and secondary fluorescence enhancement induced by hard X-rays of the same and neighboring layers.

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