Artigo Revisado por pares

Synthesis and structural characterization of Ba(LnIII2/3BVI1/3)O3 (LnIII=Dy, Gd and Sm; BVI=Mo or W) complex perovskites

2003; Elsevier BV; Volume: 175; Issue: 2 Linguagem: Inglês

10.1016/s0022-4596(03)00291-3

ISSN

1095-726X

Autores

Antonio F. Fuentes, M. Garza-Garcı́a, J.I. Escalante-Garcı́a, G. Mendoza-Suárez, Khalid Boulahya, Ulises Amador,

Tópico(s)

Advanced Condensed Matter Physics

Resumo

Abstract We describe in this work the synthesis and crystal structure of five rare earth and Mo(VI) or W(VI) containing complex perovskites. The compounds studied are Ba(Dy 2/3 Mo 1/3 )O 3 , Ba(Dy 2/3 W 1/3 )O 3 , Ba(Gd 2/3 Mo 1/3 )O 3 , Ba(Gd 2/3 W 1/3 )O 3 and Ba(Sm 2/3 W 1/3 )O 3 and were prepared starting from solutions, by the polymeric precursors method. Structural characterization by HREM, SAED and powder XRD revealed the five compounds to be ordered cubic perovskites, SG Fm -3 m (225), with a cell parameter double of that of a simple perovskite cell and increasing as the size of the trivalent lanthanide ion increases (Dy

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