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A Layered Nickel Succinate with Unprecedented Hexanickel Units: Structure Elucidation from Powder‐Diffraction Data, and Magnetic and Sorption Properties

2003; Wiley; Volume: 42; Issue: 6 Linguagem: Inglês

10.1002/anie.200390177

1521-3773

Nathalie Guillou, Carine Livage, Wouter van Beek, Marc Noguès, Gérard Férey,

Chemical Synthesis and Characterization

Angewandte Chemie International EditionVolume 42, Issue 6 p. 643-647 Communication A Layered Nickel Succinate with Unprecedented Hexanickel Units: Structure Elucidation from Powder-Diffraction Data, and Magnetic and Sorption Properties† Nathalie Guillou Dr., Nathalie Guillou Dr. guillou@chimie.uvsq.fr Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this authorCarine Livage Dr., Carine Livage Dr. Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this authorWouter van Beek Dr., Wouter van Beek Dr. SNBL at ESRF, 6 Rue Jules Horowitz, 38043 Grenoble, FranceSearch for more papers by this authorMarc Noguès Dr., Marc Noguès Dr. Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this authorGérard Férey Prof., Gérard Férey Prof. Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this author Nathalie Guillou Dr., Nathalie Guillou Dr. guillou@chimie.uvsq.fr Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this authorCarine Livage Dr., Carine Livage Dr. Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this authorWouter van Beek Dr., Wouter van Beek Dr. SNBL at ESRF, 6 Rue Jules Horowitz, 38043 Grenoble, FranceSearch for more papers by this authorMarc Noguès Dr., Marc Noguès Dr. Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this authorGérard Férey Prof., Gérard Férey Prof. Institut Lavoisier-Franklin, FR 2483, Université de Versailles Saint-Quentin-en-Yvelines, 45 avenue des Etats-Unis, 78035 Versailles Cedex, France, Fax: (+33) 1-3925-4358Search for more papers by this author First published: 06 February 2003 https://doi.org/10.1002/anie.200390177Citations: 43 † We thank the ESRF for allowing us access to their synchrotron facilities. Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat Graphical Abstract Despite the presence of 55 nonequivalent atoms the structure of the layered nickel succinate [Ni7(C4H4O4)4(OH)6(H2O)3]⋅7 H2O was solved by ab initio methods from powder-diffraction data. The structure contains unprecedented Ni6 units (blue in the picture) linked by further Ni-centered octahedra (green) and succinate ions (yellow). Citing Literature Supporting Information Supporting information for this article is available on the WWW under http://www.wiley-vch.de/contents/jc_2002/2003/z50247_s.pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. Volume42, Issue6February 10, 2003Pages 643-647 RelatedInformation