Is Enantiomer Assignment Possible by NMR Spectroscopy Using Residual Dipolar Couplings from Chiral Nonracemic Alignment Media?

Artigo Revisado por pares

Is Enantiomer Assignment Possible by NMR Spectroscopy Using Residual Dipolar Couplings from Chiral Nonracemic Alignment Media?—A Critical Assessment

2012; Wiley; Volume: 51; Issue: 33 Linguagem: Inglês

10.1002/anie.201107626

ISSN

1521-3773

Autores

Robert Berger, Jacques Courtieu, Roberto R. Gil, Christian Griesinger, Matthias Köck, Philippe Lesot, Burkhard Luy, Denis Merlet, Armando Navarro‐Vázquez, Michael Reggelin, Uwe M. Reinscheid, Christina M. Thiele, Markus Zweckstetter,

Tópico(s)

Metabolomics and Mass Spectrometry Studies

Resumo

Insensitive towards inversion: Can residual dipolar couplings (RDCs) and other anisotropic NMR observables be used to determine absolute configuration? A critical assessment of recent approaches is provided to determine the absolute configuration from RDCs.

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Is Enantiomer Assignment Possible by NMR Spectroscopy Using Residual Dipolar Couplings from Chiral Nonracemic Alignment Media?—A Critical Assessment