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High-resolution solid-state MAS73Ge NMR spectra of some organogermanes

2005; Wiley; Volume: 43; Issue: 8 Linguagem: Inglês

10.1002/mrc.1603

1097-458X

Yoshito Takeuchi, Miki Nishikawa, Houjin Hachiya, Hiroshi Yamamoto,

Organoboron and organosilicon chemistry

Magnetic Resonance in ChemistryVolume 43, Issue 8 p. 662-664 Note High-resolution solid-state MAS 73Ge NMR spectra of some organogermanes Yoshito Takeuchi, Corresponding Author Yoshito Takeuchi [email protected] Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, Japan2-26-9 Kohinata, Bunkyo-ku, Tokyo 112-0006, Japan.===Search for more papers by this authorMiki Nishikawa, Miki Nishikawa Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, JapanSearch for more papers by this authorHoujin Hachiya, Houjin Hachiya Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, JapanSearch for more papers by this authorHiroshi Yamamoto, Hiroshi Yamamoto Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, JapanSearch for more papers by this author Yoshito Takeuchi, Corresponding Author Yoshito Takeuchi [email protected] Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, Japan2-26-9 Kohinata, Bunkyo-ku, Tokyo 112-0006, Japan.===Search for more papers by this authorMiki Nishikawa, Miki Nishikawa Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, JapanSearch for more papers by this authorHoujin Hachiya, Houjin Hachiya Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, JapanSearch for more papers by this authorHiroshi Yamamoto, Hiroshi Yamamoto Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi 259-1293, JapanSearch for more papers by this author First published: 25 May 2005 https://doi.org/10.1002/mrc.1603Citations: 11AboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onEmailFacebookTwitterLinkedInRedditWechat Abstract High-resolution solid-state magic angle spinning 73Ge NMR spectra of some organogermanium compounds were measured. Most tetrasubstituted germanes with identical substituents exhibited signals except for one case. Tetrasubstituted germanes with two kinds of different but somewhat similar substituents exhibited broad peaks. Trisubstituted germanes failed to show signals, indicating the importance of symmetry around germanium. Copyright © 2005 John Wiley & Sons, Ltd. REFERENCES 1Takeuchi Y, Nishikawa M, Tanaka K, Takayama T, Imanari I, Deguchi K, Sugisawa Y. J. Chem. Soc., Chem. Commun. 2000; 687. 2Takeuchi Y, Nishikawa M, Tanaka K. Chem. Lett. 2001; 372. 3Takeuchi Y, Takayama T. Annu. Rep. NMR Spectosc. 2005; 54: 155. 4Eaborn C, Singh B. J. Organomet. Chem. 1979; 177: 333. 5Klaukien H, Lehnig M, Reiche T, Reib S, Such P. J. Chem. Soc., Perkin Trans. 2 1995; 2119. 6Takeuchi Y, Yamamoto H, Tanaka K, Ogawa O, Harada J, Iwamoto T, Yuge H. Tetrahedron 1998; 54: 9811. 7(a) Tamborski C. US Patent 3 392 178, 1968; (b) Kulikova TI, Makarenko NP, Yashin YI. Zh. Fiz. Khim. 2003; 77: 1297. 8Roberts RMG. J. Organomet. Chem. 1973; 63: 159. 9Charisse M, Zickgral A, Stemger H, Brau E, Desmaquet C, Dräger M, Gerstmann S, Daketernieks D, Hook J. Polyhedron 1998; 17: 4497. Citing Literature Volume43, Issue8August 2005Pages 662-664 ReferencesRelatedInformation