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Continuous In Situ Generation, Separation, and Reaction of Diazomethane in a Dual‐Channel Microreactor

2011; Wiley; Volume: 50; Issue: 26 Linguagem: Inglês

10.1002/anie.201101977

1521-3773

Ram Awatar Maurya, Chan Pil Park, Jang Han Lee, Dong‐Pyo Kim,

Analytical Chemistry and Chromatography

A fierce dog: A method for the continuous in-situ on-demand generation, separation, and reaction of diazomethane in a dual-channel microreactor has been developed (see picture; Diazald=N-methyl-N-nitroso-p-toluenesulfonamide). The microchemical system allows a variety of diazomethane reactions to be performed without the most common problems of preparation, handling, transfer, and decomposition. Detailed facts of importance to specialist readers are published as "Supporting Information". Such documents are peer-reviewed, but not copy-edited or typeset. They are made available as submitted by the authors. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article.