Portal de Periódicos da CAPES

Synthesis and characterization of 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride

1999; Elsevier BV; Volume: 40; Issue: 29 Linguagem: Inglês

10.1016/s0040-4039(99)00968-5

1873-3581

Munetaka Kunishima, Chiho Kawachi, Fumiaki Iwasaki, Keiji Terao, Shohei Tani,

Chemical Reaction Mechanisms

4-(4,6-Dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride (DMTMM) was quantitatively synthesized by the coupling of 2-chloro-4,6-dimethoxy-1,3,5-triazine and N-methylmorpholine in THF, and fully characterized. Condensation of car☐ylic acids and amines by DMTMM proceeded effectively in THF to give the corresponding amides in good yield.