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Molecular Iodine-Catalyzed Facile Procedure for N -Boc Protection of Amines

2006; American Chemical Society; Volume: 71; Issue: 21 Linguagem: Inglês

10.1021/jo0612473

1520-6904

Ravi Varala, Sreelatha Nuvula, Srinivas R. Adapa,

Oxidative Organic Chemistry Reactions

An efficient and practical protocol for the protection of various structurally and electronically divergent aryl and aliphatic amines using (Boc)2O in the presence of a catalytic amount of molecular iodine (10 mol %) under solvent-free conditions at ambient temperature is presented.