Modern solid state NMR techniques and concepts in structural studies of synthetic polymers
2016; Wiley; Volume: 27; Issue: 9 Linguagem: Inglês
10.1002/pat.3780
ISSN1099-1581
AutoresSławomir Kaźmierski, Tomasz Pawlak, Agata Jeziorna, Marek J. Potrzebowski,
Tópico(s)NMR spectroscopy and applications
ResumoPolymers for Advanced TechnologiesVolume 27, Issue 9 p. 1143-1155 Review Modern solid state NMR techniques and concepts in structural studies of synthetic polymers S. Kaźmierski, S. Kaźmierski The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, PolandSearch for more papers by this authorT. Pawlak, T. Pawlak The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, PolandSearch for more papers by this authorA. Jeziorna, A. Jeziorna The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, PolandSearch for more papers by this authorM. J. Potrzebowski, Corresponding Author M. J. Potrzebowski The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, Poland Correspondence to: Marek J. Potrzebowski, Center of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, 90-363 Łódź, Poland.E-mail: marekpot@cbmm.lodz.plSearch for more papers by this author S. Kaźmierski, S. Kaźmierski The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, PolandSearch for more papers by this authorT. Pawlak, T. Pawlak The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, PolandSearch for more papers by this authorA. Jeziorna, A. Jeziorna The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, PolandSearch for more papers by this authorM. J. Potrzebowski, Corresponding Author M. J. Potrzebowski The Centre of Molecular and Macromolecular Studies, Polish Academy of Science, Łódź, Poland Correspondence to: Marek J. Potrzebowski, Center of Molecular and Macromolecular Studies, Polish Academy of Sciences, Sienkiewicza 112, 90-363 Łódź, Poland.E-mail: marekpot@cbmm.lodz.plSearch for more papers by this author First published: 24 February 2016 https://doi.org/10.1002/pat.3780Citations: 10Read the full textAboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat Abstract In this mini-review, we present the solid state nuclear magnetic resonance (NMR) methods which trace the new tendency in structural studies of synthetic polymers. The review is organized into three sections. In the first part, short theoretical background and introduction to very fast magic angle spinning NMR technique with sample rotation 60 kHz are shown. The second part presents method for enhancing the sensitivity of NMR experiments by application of dynamic nuclear polarization magic angle spinning technique. In the third section, the power of the NMR crystallography approach which can be used for fine refinement of polymers structure on the atomic level is discussed. Copyright © 2016 John Wiley & Sons, Ltd. Citing Literature Volume27, Issue9September 2016Pages 1143-1155 RelatedInformation
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