Solid-state mechanochemical conversion of one-dimensional pencil shaped sodium coordination polymer nanorods to corrugated tape silver coordination polymer nanoparticles
2017; Elsevier BV; Volume: 82; Linguagem: Inglês
10.1016/j.inoche.2017.05.004
ISSN1879-0259
AutoresFatemeh Shahangi Shirazi, Kamran Akhbari, Jaursup Boonmak, Sujittra Youngme,
Tópico(s)Dendrimers and Hyperbranched Polymers
ResumoIrreversible solid-state conversion of pencil shaped Na coordination polymer nanorods, prepared by sonochemical procedure, to nanoparticles of corrugated tape silver polymer has been observed upon mechanochemical reaction of compound [Na(μ2-Hdcpa)(μ3-dcpa)]n (1), [Hdcpa = 2,4-dichlorophenoxyacetic acid] with AgNO3. These nanostructures were characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRD), IR spectroscopy and elemental analyses. Thermal stability of these samples was also studied by thermo gravimetric (TG) and differential thermal analyses (DTA).
Referência(s)