Artigo Acesso aberto Revisado por pares

Structure of the SnO 2 ( 110 ) − ( 4 × 1 ) Surface

2017; American Physical Society; Volume: 119; Issue: 9 Linguagem: Inglês

10.1103/physrevlett.119.096102

ISSN

1092-0145

Autores

Lindsay R. Merte, Mathias Jørgensen, K. Pussi, Johan Gustafson, Mikhail Shipilin, Andreas Schaefer, Chu Zhang, Jonathan Rawle, Chris Nicklin, G. Thornton, R. Lindsay, Bjørk Hammer, Edvin Lundgren,

Tópico(s)

ZnO doping and properties

Resumo

Using surface x-ray diffraction (SXRD), quantitative low-energy electron diffraction (LEED), and density-functional theory (DFT) calculations, we have determined the structure of the ($4\ifmmode\times\else\texttimes\fi{}1$) reconstruction formed by sputtering and annealing of the ${\mathrm{SnO}}_{2}(110)$ surface. We find that the reconstruction consists of an ordered arrangement of ${\mathrm{Sn}}_{3}{\mathrm{O}}_{3}$ clusters bound atop the bulk-terminated ${\mathrm{SnO}}_{2}(110)$ surface. The model was found by application of a DFT-based evolutionary algorithm with surface compositions based on SXRD, and shows excellent agreement with LEED and with previously published scanning tunneling microscopy measurements. The model proposed previously consisting of in-plane oxygen vacancies is thus shown to be incorrect, and our result suggests instead that Sn(II) species in interstitial positions are the more relevant features of reduced ${\mathrm{SnO}}_{2}(110)$ surfaces.

Referência(s)