Synthesis and characterization of ZnO–CuO nanocomposites powder by modified perfume spray pyrolysis method and its antimicrobial investigation
2018; IOP Publishing; Volume: 39; Issue: 3 Linguagem: Inglês
10.1088/1674-4926/39/3/033001
ISSN2058-6140
AutoresD. Saravanakkumar, S. Sivaranjani, K. Kaviyarasu, A. Ayeshamariam, B. Ravikumar, S. Pandiarajan, C. Veeralakshmi, M. Jayachandran, M. Mâaza,
Tópico(s)Gas Sensing Nanomaterials and Sensors
ResumoPure ZnO, ZnO–CuO nanocomposites can be synthesized by using a modified perfume spray pyrolysis method (MSP). The crystallite size of the nanoparticles (NPs) has been observed by X-ray diffraction pattern and is nearly 36 nm. Morphological studies have been analyzed by using Field Emission Scanning Electron Microscopy (FESEM) and its elemental analysis was reported by Elemental X-ray Analysis (EDX); these studies confirmed that ZnO and CuO have hexagonal structure and monoclinic structure respectively. Fourier Transform Infrared (FTIR) spectra revealed that the presence of functional frequencies of ZnO and CuO were observed at 443 and 616 cm−1. The average bandgap value at 3.25 eV using UV–vis spectra for the entitled composite has described a blue shift that has been observed here. The antibacterial study against both gram positive and negative bacteria has been studied by the disc diffusion method. To the best of our knowledge, it is the first report on ZnO–CuO nanocomposite synthesized by a modified perfume spray pyrolysis method.
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