Artigo Revisado por pares

HOBt and HOAt-derived immonium salts: new and highly efficient coupling reagents for peptide synthesis

2000; Elsevier BV; Volume: 41; Issue: 5 Linguagem: Inglês

10.1016/s0040-4039(99)02125-5

ISSN

1873-3581

Autores

Peng Li, Jie‐Cheng Xu,

Tópico(s)

Biochemical and Structural Characterization

Resumo

Novel HOBt- and HOAt-derived immonium type coupling reagents BDMP, BPMP and AOMP were shown to be very efficient for peptide synthesis with high reactivity, low racemization and good yields. X-Ray analysis indicates BOMI exists as the N-substituted form rather than as the O-substituted form assigned previously. A mechanism for amide bond formation mediated by these reagents was proposed and studied.

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