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A facile synthesis of cyclic enecarbamates using Dess–Martin periodinane

2001; Elsevier BV; Volume: 42; Issue: 31 Linguagem: Inglês

10.1016/s0040-4039(01)00998-4

1873-3581

Chengzhi Yu, Longqin Hu,

Asymmetric Synthesis and Catalysis

A simple and efficient synthesis of cyclic enecarbamates from ω-hydroxycarbamates via tandem oxidative cyclization–dehydration was achieved in 84% to quantitative yield using Dess–Martin periodinane in methylene chloride.