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Solvent Free Synthetic Procedure throughout Reaction and Separation: Ylide Reaction with Alkyl Aryl Ketones in the Absence of Solvent Followed by Distillation to Give 1-Alkyl-1-aryloxiranes

1997; Elsevier BV; Volume: 46; Issue: 1 Linguagem: Inglês

10.3987/com-97-s69

1881-0942

F. Toda, Kazuyuki Kanemoto,

Chemical Reaction Mechanisms

After heating a mixture of trimethylsulphonium iodide, t BuOK and an alkyl aryl ketone at 60-70 "C for 1-5 h, vacuum distillation gave