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Hydrodeoxygenation of vegetable oil in batch reactor: Experimental considerations

2020; Elsevier BV; Volume: 28; Issue: 6 Linguagem: Inglês

10.1016/j.cjche.2019.12.022

2210-321X

Alexis K. Noriega, Alexis Tirado, Cecilia Méndez, Gustavo Marroquín, Jorge Ancheyta,

Catalysis for Biomass Conversion

The generation of reliable experimental data in any experimental scale requires proper procedures not only for the reaction step but also for the feed preparation, separation, and characterization of products as well as calculations of conversion and product yields. Batch reactor is the most used experimental setup for carrying out exploratory studies for catalyst screening and development. This work is focused on describing and discussing a step-by-step methodology for conducting experiments for catalytic hydrotreating of vegetable oils in batch reactor. The proposed methodology considers literature and own experiences on advantages and disadvantages of different feed types, catalysts, experimental setup and procedures, effect of reaction parameters, separation and characterization of products, and calculations.