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Monitoring off-resonance signals with SHARPER NMR – the MR-SHARPER experiment

2022; Royal Society of Chemistry; Volume: 147; Issue: 8 Linguagem: Inglês

10.1039/d2an00134a

1364-5528

Matthew Davy, Claire L. Dickson, Wei Ran, Dušan Uhrı́n, Craig P. Butts,

Molecular spectroscopy and chirality

We extend the SHARPER NMR method designed to accommodate challenging reaction conditions to monitor simultaneously multiple resonances such as those of a reactant (2,6-difluoro-4-methoxyphenylboronic acid) and product (3,5-difluoroanisole).