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A DMSO‐Compatible Orienting Medium: Towards the Investigation of the Stereochemistry of Natural Products

2004; Wiley; Volume: 117; Issue: 3 Linguagem: Inglês

10.1002/ange.200461267

1521-3757

Peter Haberz, Jonathan Farjon, Christian Griesinger,

Advanced NMR Techniques and Applications

Angewandte ChemieVolume 117, Issue 3 p. 431-433 Zuschrift A DMSO-Compatible Orienting Medium: Towards the Investigation of the Stereochemistry of Natural Products† Correction(s) for this article A DMSO-Compatible Orienting Medium: Towards the Investigation of the Stereochemistry of Natural Products Peter Haberz Mag., Jonathan Farjon Dr., Christian Griesinger Prof. Dr., Volume 119Issue 41Angewandte Chemie pages: 7874-7874 First Published online: October 4, 2007 Peter Haberz Mag., Peter Haberz Mag. Max Planck Institut for Biophysical Chemistry, Abt. 030: NMR-Based Structural Biology, Am Fassberg 11, 37 077 Göttingen, Germany, Fax: (+49) 551-201-2202Search for more papers by this authorJonathan Farjon Dr., Jonathan Farjon Dr. Max Planck Institut for Biophysical Chemistry, Abt. 030: NMR-Based Structural Biology, Am Fassberg 11, 37 077 Göttingen, Germany, Fax: (+49) 551-201-2202Search for more papers by this authorChristian Griesinger Prof. Dr., Christian Griesinger Prof. Dr. cigr@nmr.mpibpc.mpg.de Max Planck Institut for Biophysical Chemistry, Abt. 030: NMR-Based Structural Biology, Am Fassberg 11, 37 077 Göttingen, Germany, Fax: (+49) 551-201-2202Search for more papers by this author Peter Haberz Mag., Peter Haberz Mag. Max Planck Institut for Biophysical Chemistry, Abt. 030: NMR-Based Structural Biology, Am Fassberg 11, 37 077 Göttingen, Germany, Fax: (+49) 551-201-2202Search for more papers by this authorJonathan Farjon Dr., Jonathan Farjon Dr. Max Planck Institut for Biophysical Chemistry, Abt. 030: NMR-Based Structural Biology, Am Fassberg 11, 37 077 Göttingen, Germany, Fax: (+49) 551-201-2202Search for more papers by this authorChristian Griesinger Prof. Dr., Christian Griesinger Prof. Dr. cigr@nmr.mpibpc.mpg.de Max Planck Institut for Biophysical Chemistry, Abt. 030: NMR-Based Structural Biology, Am Fassberg 11, 37 077 Göttingen, Germany, Fax: (+49) 551-201-2202Search for more papers by this author First published: 29 December 2004 https://doi.org/10.1002/ange.200461267Citations: 50 † This work was supported by the DFG (SFB 472-Z-project), the Max Planck Gesellschaft, and the Fonds der Chemischen Industrie. J.F. is supported by a grant from the DAAD. We are grateful to Markus Radzom and Axel Zeeck for providing the hormaomycin, to Uwe Reinscheid for help with the hormaomycin spectra, to Hui Geng and Heike Neubauer for the preparation of the decasaccharide, to Christophe Farès and Jochen Junker for useful editorial advice, as well as to Markus Zweckstetter for very helpful discussions concerning the program PALES. Read the full textAboutPDF ToolsRequest permissionAdd to favorites ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinkedInRedditWechat Graphical Abstract Organische Moleküle unterschiedlicher Komplexität werden durch ein DMSO-kompatibles Gel so ausgerichtet, dass dipolare C-H-Kopplungen bis 29 Hz beobachtbar sind. Dies ebnet den Weg zur simultanen NMR-spektroskopischen Bestimmung der Konformation und Konfiguration organischer Verbindungen und somit der Stereochemie von Naturstoffen, die nicht kristallisiert werden können (z. B. Hormaomycin, siehe Bild). Citing Literature Supporting Information Supporting information for this article is available on the WWW under http://www.wiley-vch.de/contents/jc_2001/2005/z461267_s.pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. Volume117, Issue3January 7, 2005Pages 431-433 This is the German version of Angewandte Chemie. Note for articles published since 1962: Do not cite this version alone. Take me to the International Edition version with citable page numbers, DOI, and citation export. We apologize for the inconvenience. RelatedInformation