Synthesis of a Novel Zeolite through a Pressure‐Induced Reconstructive Phase Transition Process
2013; Wiley; Volume: 125; Issue: 40 Linguagem: Inglês
10.1002/ange.201305230
ISSN1521-3757
AutoresJ.L. Jordá, Fernando Rey, Germán Sastre, Susana Valencia, Miguel Palomino, Avelino Corma, A. Segura, Daniel Errandonea, Raúl Lacomba, F. J. Manjón, O. Gomis, Annette Kleppe, A. P. Jephcoat, M. Amboage, J. Alberto Rodríguez‐Velamazán,
Tópico(s)Metal-Organic Frameworks: Synthesis and Applications
ResumoAngewandte ChemieVolume 125, Issue 40 p. 10652-10656 Zuschrift Synthesis of a Novel Zeolite through a Pressure-Induced Reconstructive Phase Transition Process† Dr. Jose L. Jordá, Dr. Jose L. Jordá Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorProf. Fernando Rey, Prof. Fernando Rey Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorDr. German Sastre, Dr. German Sastre Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorDr. Susana Valencia, Dr. Susana Valencia Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorMiguel Palomino, Miguel Palomino Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorProf. Avelino Corma, Corresponding Author Prof. Avelino Corma [email protected] Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorProf. Alfredo Segura, Prof. Alfredo Segura Instituto de Ciencia de Materiales de la Universidad de Valencia, MALTA Consolider Team, Universidad de Valencia, C. Dr. Moliner 50, 46100 Burjassot (Spain)Search for more papers by this authorProf. Daniel Errandonea, Prof. Daniel Errandonea Instituto de Ciencia de Materiales de la Universidad de Valencia, MALTA Consolider Team, Universidad de Valencia, C. Dr. Moliner 50, 46100 Burjassot (Spain)Search for more papers by this authorDr. Raúl Lacomba, Dr. Raúl Lacomba Instituto de Ciencia de Materiales de la Universidad de Valencia, MALTA Consolider Team, Universidad de Valencia, C. Dr. Moliner 50, 46100 Burjassot (Spain)Search for more papers by this authorProf. Francisco J. Manjón, Prof. Francisco J. Manjón Instituto de Diseño para la Fabricación y Producción Automatizada, MALTA Consolider Team, Universidad Politécnica de Valencia, Cno. de Vera, s/n, 46022 Valencia (Spain)Search for more papers by this authorDr. Óscar Gomis, Dr. Óscar Gomis Centro de Tecnologías Físicas: Acústica, Materiales y Astrofísica, MALTA Consolider Team, Universidad Politécnica de Valencia, Cno. de Vera, s/n, 46022 Valencia (Spain)Search for more papers by this authorDr. Annette K. Kleppe, Dr. Annette K. Kleppe DIAMOND Light Source, Harwell Science and Innovation Campus, Didcot (UK)Search for more papers by this authorProf. Andrew P. Jephcoat, Prof. Andrew P. Jephcoat DIAMOND Light Source, Harwell Science and Innovation Campus, Didcot (UK) Department of Earth Sciences, University of Oxford, South Parks Road, Oxford, OX1 3AN (UK)Search for more papers by this authorDr. Mónica Amboage, Dr. Mónica Amboage DIAMOND Light Source, Harwell Science and Innovation Campus, Didcot (UK)Search for more papers by this authorDr. J. Alberto Rodríguez-Velamazán, Dr. J. Alberto Rodríguez-Velamazán Instituto de Ciencia de Materiales de Aragón (CSIC-Universidad de Zaragoza) at Institute Laue-Langevin, Grenoble (France)Search for more papers by this author Dr. Jose L. Jordá, Dr. Jose L. Jordá Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorProf. Fernando Rey, Prof. Fernando Rey Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorDr. German Sastre, Dr. German Sastre Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorDr. Susana Valencia, Dr. Susana Valencia Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorMiguel Palomino, Miguel Palomino Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorProf. Avelino Corma, Corresponding Author Prof. Avelino Corma [email protected] Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Instituto de Tecnología Química (UPV-CSIC), Universidad Politécnica de Valencia-Consejo Superior de Investigaciones Científicas, Av. de los Naranjos s/n 46022 Valencia (Spain)Search for more papers by this authorProf. Alfredo Segura, Prof. Alfredo Segura Instituto de Ciencia de Materiales de la Universidad de Valencia, MALTA Consolider Team, Universidad de Valencia, C. Dr. Moliner 50, 46100 Burjassot (Spain)Search for more papers by this authorProf. Daniel Errandonea, Prof. Daniel Errandonea Instituto de Ciencia de Materiales de la Universidad de Valencia, MALTA Consolider Team, Universidad de Valencia, C. Dr. Moliner 50, 46100 Burjassot (Spain)Search for more papers by this authorDr. Raúl Lacomba, Dr. Raúl Lacomba Instituto de Ciencia de Materiales de la Universidad de Valencia, MALTA Consolider Team, Universidad de Valencia, C. Dr. Moliner 50, 46100 Burjassot (Spain)Search for more papers by this authorProf. Francisco J. Manjón, Prof. Francisco J. Manjón Instituto de Diseño para la Fabricación y Producción Automatizada, MALTA Consolider Team, Universidad Politécnica de Valencia, Cno. de Vera, s/n, 46022 Valencia (Spain)Search for more papers by this authorDr. Óscar Gomis, Dr. Óscar Gomis Centro de Tecnologías Físicas: Acústica, Materiales y Astrofísica, MALTA Consolider Team, Universidad Politécnica de Valencia, Cno. de Vera, s/n, 46022 Valencia (Spain)Search for more papers by this authorDr. Annette K. Kleppe, Dr. Annette K. Kleppe DIAMOND Light Source, Harwell Science and Innovation Campus, Didcot (UK)Search for more papers by this authorProf. Andrew P. Jephcoat, Prof. Andrew P. Jephcoat DIAMOND Light Source, Harwell Science and Innovation Campus, Didcot (UK) Department of Earth Sciences, University of Oxford, South Parks Road, Oxford, OX1 3AN (UK)Search for more papers by this authorDr. Mónica Amboage, Dr. Mónica Amboage DIAMOND Light Source, Harwell Science and Innovation Campus, Didcot (UK)Search for more papers by this authorDr. J. Alberto Rodríguez-Velamazán, Dr. J. Alberto Rodríguez-Velamazán Instituto de Ciencia de Materiales de Aragón (CSIC-Universidad de Zaragoza) at Institute Laue-Langevin, Grenoble (France)Search for more papers by this author First published: 01 August 2013 https://doi.org/10.1002/ange.201305230Citations: 16 † We thank the Diamond Light Source (beamline I15) and Institute Laue-Langevin (beamline D1B) for beamtime allocation, and the Spanish Government (projects MAT2010-21270-C04-01/04, MAT-2012-3856-C02-01, CTQ2010-17988/PPQ, Consolider MALTA CSD-2007-00045, Consolider Ingenio Multicat CSD-2009-00050 and program Severo Ochoa SEV-2012-0267), Generalitat Valenciana (Project Prometeo and GVA-acomp-2013-012) and "Vicerrectorado de Innovación y Desarrollo de la UPV" (PAID-05-2009, project UPV2010-0096) for financial support. G.S. thanks Centro de Cálculo (UPV) and Área de Informática Científica (SGAI-CSIC) for Computational facilities. We thank Dr. Vidal-Moya for 29Si-MAS-NMR measurements and T. Portilla for technical support. Read the full textAboutPDF ToolsRequest permissionAdd to favorites ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onEmailFacebookTwitterLinkedInRedditWechat Graphical Abstract Durch Druckeinwirkung auf den herkömmlichen Zeolith ITQ-29 gelang erstmals die druckinduzierte Festphasensynthese eines Zeoliths (siehe Schema; Si gelb, O rot): Das Produkt, ITQ-50, hat eine einzigartige mikroporöse Struktur und ist leistungsfähiger in der Propen-Propan-Trennung als das Ausgangsmaterial ITQ-29. Supporting Information As a service to our authors and readers, this journal provides supporting information supplied by the authors. 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