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Attrition‐Enhanced Deracemization of an Amino Acid Derivative That Forms an Epitaxial Racemic Conglomerate

2008; Wiley; Volume: 120; Issue: 38 Linguagem: Alemão

10.1002/ange.200802468

1521-3757

Bernard Kaptein, Wim L. Noorduin, Hugo Meekes, W.J.P. van Enckevort, Richard M. Kellogg, Elias Vlieg,

Protein Structure and Dynamics

Angewandte ChemieVolume 120, Issue 38 p. 7336-7339 Zuschrift Attrition-Enhanced Deracemization of an Amino Acid Derivative That Forms an Epitaxial Racemic Conglomerate† Bernard Kaptein Dr., Bernard Kaptein Dr. bernard.kaptein@dsm.com Innovative Synthesis & Catalysis, DSM Pharmaceutical Products, PO Box 18, 6160 MD Geleen (The Netherlands), Fax: (+31) 46-476-7604Search for more papers by this authorWim L. Noorduin, Wim L. Noorduin IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this authorHugo Meekes Dr., Hugo Meekes Dr. IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this authorWillem J. P. van Enckevort Dr., Willem J. P. van Enckevort Dr. IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this authorRichard M. Kellogg Prof. Dr., Richard M. Kellogg Prof. Dr. r.m.kellogg@syncom.nl Syncom BV, Kadijk 3, 9747 AT Groningen (The Netherlands), Fax: (+31) 50-575-399Search for more papers by this authorElias Vlieg Prof. Dr., Elias Vlieg Prof. Dr. e.vlieg@science.ru.nl IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this author Bernard Kaptein Dr., Bernard Kaptein Dr. bernard.kaptein@dsm.com Innovative Synthesis & Catalysis, DSM Pharmaceutical Products, PO Box 18, 6160 MD Geleen (The Netherlands), Fax: (+31) 46-476-7604Search for more papers by this authorWim L. Noorduin, Wim L. Noorduin IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this authorHugo Meekes Dr., Hugo Meekes Dr. IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this authorWillem J. P. van Enckevort Dr., Willem J. P. van Enckevort Dr. IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this authorRichard M. Kellogg Prof. Dr., Richard M. Kellogg Prof. Dr. r.m.kellogg@syncom.nl Syncom BV, Kadijk 3, 9747 AT Groningen (The Netherlands), Fax: (+31) 50-575-399Search for more papers by this authorElias Vlieg Prof. Dr., Elias Vlieg Prof. Dr. e.vlieg@science.ru.nl IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, 6525 AJ Nijmegen (The Netherlands), Fax: (+31) 24-365-3067Search for more papers by this author First published: 03 September 2008 https://doi.org/10.1002/ange.200802468Citations: 43 † J. M. M. Smits is acknowledged for performing the X-ray single-crystal structure determination. The SNN agency (Cooperation Northern Netherlands) and the European Fund for Regional Development (EFRO) are acknowledged for partial financial support of this research. Read the full textAboutPDF ToolsRequest permissionAdd to favorites ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL Share a linkShare onFacebookTwitterLinked InRedditWechat Abstract Trotz epitaktischem Verhalten der Enantiomere gelang die vollständige Enantiomerentrennung des gezeigten Phenylalaninderivats durch Scheuermahlen von Kristallen der Verbindung in einer gesättigten racemisierenden Lösung. Ostwald-Reifung spielt eine wichtige Rolle in diesem Prozess, wie die Untersuchung des Einflusses der Kristallgröße ergab. Citing Literature Supporting Information Supporting information for this article is available on the WWW under http://www.wiley-vch.de/contents/jc_2001/2008/z802468_s.pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article. Volume120, Issue38September 8, 2008Pages 7336-7339 This is the German version of Angewandte Chemie. Note for articles published since 1962: Do not cite this version alone. Take me to the International Edition version with citable page numbers, DOI, and citation export. We apologize for the inconvenience. RelatedInformation