Artigo Produção Nacional Revisado por pares

Physicochemical properties of calcium silicate cement based endodontic sealers

2024; Elsevier BV; Volume: 151; Linguagem: Inglês

10.1016/j.jmbbm.2024.106400

ISSN

1751-6161

Autores

Sérgio André Lopes Quaresma, Guilherme Nilson Alves dos Santos, Alice Corrêa Silva‐Sousa, Rafael Verardino de Camargo, Fabiane Carneiro Lopes‐Olhê, Yara Teresinha Corrêa Silva‐Sousa, Jardel Francisco Mazzi‐Chaves, Manoel Damião Sousa‐Neto,

Tópico(s)

Dental materials and restorations

Resumo

To mensure the physicochemical properties of three ceramic cement endodontic sealers AH Plus Bioceramic, Bio-C Sealer and Bio-C Sealer Ion+ with an epoxy resin sealer, AH Plus. These properties were measured: hardening time (HT), dimensional change (DC), solubility (SL), flow (FL) and radiopacity (RD). The distilled water obtained from the SL test was analyzed with atomic absorption spectrometry. A sample calculation was made considering n = 5 repetitions for each experimental sealer evaluated. Statistical analysis was performed using one-way ANOVA and post hoc Tukey tests (p < 0.05). For the HT, AH Plus (484 ± 2.76 min) and AH Plus Bioceramic (424 ± 1.23 min) set more slowly than of Bio-C Sealer (370 ± 4.50 min) and Bio-C Sealer Ion+ (380 ± 1.42 min) (p < 0.05). AH Plus Bioceramic (12.56 ± 2.71 %) was more soluble than Bio-C Sealer (6.69 ± 1.67 %), Bio-C Sealer Ion+ (5.67 ± 2.16 %) and AH Plus (0.15 ± 0.01 %) (p < 0.05). AH Plus (0.03 ± 0.01 %) had slight expansion while the cement-based sealers had shrinkage: AH Plus Bioceramic (−1.60 ± 0.63 %) and Bio-C Sealer (−1.38 ± 0.69 %), Bio-C Sealer Ion+ (−5.19 ± 1.23 %) (p < 0.05). Bio-C Sealer Ion+ (59.80 ± 0.86 mm) and Bio-C Sealer (58.60 ± 0.98 mm) had the highest flow compared with AH Plus (56.90 ± 0.56 mm) and AH Plus Bioceramic (49.50 ± 0.63 mm) (p < 0.05). AH Plus (9.17 ± 0.06 mmAl) and AH Plus Bioceramic (8.27 ± 0.84 mmAl) showed radiopacity values when compared with those of Bio-C Sealer (4.90 ± 0.08 mmAl) and Bio-C Sealer Ion+ (4.14 ± 0.05 mmAl) (p > 0.05). Ion release is inhered to these cement-based sealers and this result in calcium ion release.

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